Details of CH3204 (Spring 2013)

Level: 3 Type: Laboratory Credits: 3.0

Course CodeCourse NameInstructor(s)
CH3204 Organic Synthesis Debasish Haldar

Syllabus
Organic Synthesis followed by purification, crystallization, UV-Vis, FTIR
and NMR characterization

1) Nitration: Preparation of 2,4-dinitroanisole from anisole
2) Acytatilation: purification of Acetanilide from aniline
3) Halogination: Preparation of p-Bromo Acetanilide from Acetanilide
4) Coupling reaction: Synthesis of methyl orrange
5) F. C. reaction: Preparation of 1,1-bis-2-napthol
6) Fischer indole synthesis: Synthesis of 2-phenyl indole from phenyl
hydrazine
7) Synthesis of 4-methyl-7-hydroxycoumarin from resorcinol and ethyl
acetoacetate
Microwave assisted synthesis: ammonium formate-mediated Knoevenagel
reaction
9) Green chemistry approach for organic synthesis: Synthesis of
dihydropyrimidinone
10) Addition elimination reaction.

References

Course Credit Options

Sl. No.ProgrammeSemester NoCourse Choice
1 IP 2 Core
2 IP 4 Not Allowed
3 MS 6 Core
4 RS 1 Elective