Details of CH3204 (Spring 2017)

Level: 3 Type: Laboratory Credits: 3.0

Course CodeCourse NameInstructor(s)
CH3204 Organic synthesis laboratory Chilla Malla Reddy,
Debasish Haldar

Syllabus
Organic Synthesis followed by purification, crystallization, UV-Vis, FTIR and NMR characterization: (1) Nitration: Preparation of 2,4-dinitroanisole from anisole, (2) Acytatilation: purification of Acetanilide from aniline, (3) Halogination: Preparation of p-Bromo Acetanilide from Acetanilide, (4) Coupling reaction: Synthesis of methyl orange, (5) F. C. reaction: Preparation of 1,1-bis-2-napthol, (6) Fischer indole synthesis: Synthesis of 2-phenyl indole from phenyl hydrazine, (7) Synthesis of 4-methyl-7-hydroxycoumarin from resorcinol and ethyl acetoacetate, (8) Microwave assisted synthesis: ammonium formate-mediated Knoevenagel reaction, (9) Green chemistry approach for organic synthesis: Synthesis of dihydropyrimidinone, (10) Addition elimination reaction, (11) Click chemistry

References

Course Credit Options

Sl. No.ProgrammeSemester NoCourse Choice
1 IP 2 Core
2 IP 4 Not Allowed
3 IP 6 Not Allowed
4 MR 2 Not Allowed
5 MR 4 Not Allowed
6 MS 6 Core
7 RS 1 Not Allowed
8 RS 2 Not Allowed