Details of CH3204 (Spring 2021)

Level: 3 Type: Laboratory Credits: 4.0

Course CodeCourse NameInstructor(s)
CH3204 Organic Synthesis Laboratory II Debasish Haldar,
Suman De Sarkar

Syllabus
Organic Synthesis followed by Purification, Crystallization, UV-Vis, FTIR and NMR
Characterization:
(1) Nitration: Preparation of 2,4-Dinitroanisole from Anisole
(2) Acetylation: Purification of Acetanilide from Aniline
(3) Halogenation: Preparation of p-Bromo Acetanilide from Acetanilide
(4) Coupling reaction: Synthesis of Methyl Orange,
(5) F. C. reaction: Preparation of 1,1-bis-2-Napthol,
(6) Fischer Indole Synthesis: Synthesis of 2-Phenylindole from Phenylhydrazine,
(7) Synthesis of 4-Methyl-7-hydroxycoumarin from Resorcinol and Ethyl acetoacetate,
(8) Microwave Assisted Synthesis: ammonium formate-mediated Knoevenagel reaction,
(9) Green Chemistry Approach in Organic Synthesis: Synthesis of Dihydropyrimidinone,
(10) Addition elimination reaction,
(11) Click chemistry.

References

Course Credit Options

Sl. No.ProgrammeSemester NoCourse Choice
1 IP 2 Not Allowed
2 IP 4 Not Allowed
3 IP 6 Not Allowed
4 MR 2 Not Allowed
5 MR 4 Not Allowed
6 MS 10 Not Allowed
7 MS 4 Not Allowed
8 MS 6 Core
9 MS 8 Not Allowed
10 RS 1 Not Allowed
11 RS 2 Not Allowed